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Samples were run in duplicate on two HPLC columns: (1) InfinityLab Poroshell 120 HILIC-Z (2.1 100 mm, 2.7 m, Agilent) with UHPLC Guard Poroshell 120 HILIC-Z (2.1 5 mm, 2.7 m, Agilent) and (2) reversed-phase ZORBAX Eclipse XDB-C18 (2.1 100 mm, 1.8 m, Agilent) with UHPLC Guard ZORBAX (2.1 5 mm, 1.8 m, Agilent)

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(American Chemical Society)Single mol

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