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The fourth aliquot was analyzed via negative ionization following elution from a HILIC column (Waters UPLC BEH Amide 2.1 mm 150 mm, 1.7 m) using a gradient consisting of water and acetonitrile with 10 mmol/L ammonium formate at pH 10.8
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+ co-transport (Figure 3 and Table 1
Sci Pharm (2015) 83:15975
