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The cis-piperidinone was epimerized to the required trans isomer using a base-catalyzed, dynamic crystallization-driven procedure, which was subsequently crystallized from the raw reaction mixture with high yield and purity
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Effects of 1 and 3 g cinnamon on gastric emptying, satiety, and postprandial blood glucose, insulin, glucose-dependent insulinotropic polypeptide, glucagon-like peptide 1, and ghrelin concentrations in healthy subjects
